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HPLC purity (typically 98-99%) measures peptide as percentage of total peptide content, but lyophilized powder contains counterions (acetate or trifluoroacetate from synthesis), residual water, and potentially buffer salts

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Takahashi K, Wang F, Morita K, Yan Y, Patel K, Bueso-Ramos CE, Gumbs C, Zhang J, Kornblau S, DiNardo CD, Ravandi F, Garcia-Manero G, Jabbour EJ, Andreeff M , Kantarjian HM, Konopleva M, Futreal A