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(2) performing gradient elution by taking a reverse-phase silica gel filler as a stationary phase, a salt solution with a pH value regulated to 7-9 by ammonia water as a mobile phase A and acetonitrile as a mobile phase B, collecting fractions, and performing rotary evaporation to remove a part of the solvent to obtain a primarily-purified solution

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J Am Coll Cardiol 44(10):19962002

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