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Nature 437 , 11091113 (2005)

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Describes general patterns observed in published research on the individual ingredients, not specific product claims

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This combined crude material was dissolved in the minimum amount of DCM, loaded onto a silica column, and eluted with a gradient of 10% EtOAc/hexanes to 39% EtOAc/hexanes to give 19.19 g of product by passage through 1H Purity as determined by NMR was approximately 95%